High resolution NMR spectroscopy
Research key trends:
̶ researchof polymer/copolymer microstructure;
̶ composition/structure characterizationandquantitationofgoal products and intermediates arisen in organic syntheses;
̶ structuralstudiesof a broad range of organic, bioorganic and natural compounds;
̶ determination of compound purity.
Instruments:
NMR spectrometer BrukerAM 50 MHz (Germany)
Probes:
1-probe 5 mmof high resolution, for liquids |
1Н ̶ 13С |
2-probe 5 mm |
1Н ̶ 19F |
3-probe 5 mm |
1Н ̶ 19F ̶ 13С |
3-broadband probe10 mm |
|
Instrument capabilities:
̶ recording1НNMRspectra 500 МHz;
̶ recording13С (125 МHz) and19F (470МHz);
̶ recordingdimensional spectraNMRin the range from 23 МHzto 500 МHz;
̶ recording spectra at various temperatures, using temperature set-top box (from -150 to +100ºС);
̶ relaxation measurements;
̶ recording NMR two-dimensional spectra COSY, NOESY.
NMRteamconsists ofhighlyskilledspecialistsable to solve a variety of research problems.Costsofservicesvary depending on work intricacy and volume.